Автор |
G K Williamson |
Автор |
A Moore |
Дата выпуска |
1956-03-01 |
dc.description |
A high-temperature specimen chamber is described in which continuous gas circulation is employed in heating a specimen 1 in. diameter × 0 020 in. thick to a uniform and accurately known temperature. Using techniques sensitive to 0.1° C no temperature differences could be detected between the centre and periphery of the specimen in the range 20-200° C and the difference had a maximum value of less than 1° C at 600° C. In practice the true temperature of the specimen can be measured throughout the range 20-650° C. Temperature fluctuations due to the control circuit never exceeded ±0.5° C as measured on the specimen. The general reliability of the chamber has been critically examined. Slight modification to the instrument should raise the maximum attainable temperature to approximately 900° C. |
Формат |
application.pdf |
Издатель |
Institute of Physics Publishing |
Название |
A precision high-temperature specimen chamber for an X-ray diffractometer |
Тип |
paper |
DOI |
10.1088/0950-7671/33/3/306 |
Print ISSN |
0950-7671 |
Журнал |
Journal of Scientific Instruments |
Том |
33 |
Первая страница |
107 |
Последняя страница |
110 |
Аффилиация |
G K Williamson; University of Birmingham |
Аффилиация |
A Moore; University of Birmingham |
Выпуск |
3 |