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Автор Liu, Yuge
Автор Zhang, Jingjing
Автор Hou, Wenhua
Автор Zhu, Jun-Jie
Дата выпуска 2008-04-02
dc.description In this paper, palladium (Pd) nanoparticles have been successfully encapsulated into the channels of modified SBA-15 in situ via a facile, ethylene glycol (EG)-assisted sonochemical method. The products were confirmed by x-ray diffraction, transmission electron microscopy (TEM) and nitrogen adsorption analysis. The Pd/SBA-15 composite was used for the realization of direct electron transfer of hemoglobin (Hb). Electrochemical results showed that the Pd nanoparticles in the channels of SBA-15 could enhance the direct electron transfer between Hb and the electrode surface. The composite modified electrode displayed excellent electrochemical behavior. The sensor fabricated by the composite showed an excellent response to the reduction of hydrogen peroxide (H<sub>2</sub>O<sub>2</sub>), and the linear range for the determination of H<sub>2</sub>O<sub>2</sub> was from 1.8 to 119.3 µM with a detection limit of 0.8 µM.
Формат application.pdf
Издатель Institute of Physics Publishing
Копирайт IOP Publishing Ltd
Название A Pd/SBA-15 composite: synthesis, characterization and protein biosensing
Тип paper
DOI 10.1088/0957-4484/19/13/135707
Electronic ISSN 1361-6528
Print ISSN 0957-4484
Журнал Nanotechnology
Том 19
Первая страница 135707
Последняя страница 135714
Аффилиация Hou, Wenhua;
Аффилиация Zhu, Jun-Jie;
Аффилиация Liu, Yuge; Key Laboratory of Mesoscopic Chemistry and Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, People’s Republic of China
Аффилиация Zhang, Jingjing; Key Laboratory of Mesoscopic Chemistry and Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, People’s Republic of China
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