| Автор | Hattrick-Simpers, Jason R |
| Автор | Tan, Zhuopeng |
| Автор | Oguchi, Hiroyuki |
| Автор | Chiu, Chun |
| Автор | Heilweil, Edwin J |
| Автор | Maslar, James E |
| Автор | Bendersky, Leonid A |
| Дата выпуска | 2011-10-01 |
| dc.description | In order to increase measurement throughput, a characterization scheme has been developed that accurately measures the hydrogen storage properties of materials in quantities ranging from 10 ng to 1 g. Initial identification of promising materials is realized by rapidly screening thin-film composition spread and thickness wedge samples using normalized IR emissivity imaging. The hydrogen storage properties of promising samples are confirmed through measurements on single-composition films with high-sensitivity (resolution <0.3 μg) Sievert's-type apparatus. For selected samples, larger quantities of up to ∼100 mg may be prepared and their (de)hydrogenation and micro-structural properties probed via parallel in situ Raman spectroscopy. Final confirmation of the hydrogen storage properties is obtained on ∼1 g powder samples using a combined Raman spectroscopy/Sievert's apparatus. |
| Формат | application.pdf |
| Издатель | Institute of Physics Publishing |
| Копирайт | 2011 National Institute for Materials Science |
| Название | A combinatorial characterization scheme for high-throughput investigations of hydrogen storage materials |
| Тип | paper |
| DOI | 10.1088/1468-6996/12/5/054207 |
| Electronic ISSN | 1878-5514 |
| Print ISSN | 1468-6996 |
| Журнал | Science and Technology of Advanced Materials |
| Том | 12 |
| Первая страница | 54207 |
| Последняя страница | 54212 |
| Аффилиация | Hattrick-Simpers, Jason R; Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA |
| Аффилиация | Tan, Zhuopeng; Department of Materials Science and Engineering, University of Maryland, College Park, MD 20742, USA |
| Аффилиация | Oguchi, Hiroyuki; Institute for Materials Research, Tohoku University, Sendai 980 8577, Japan |
| Аффилиация | Chiu, Chun; Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA |
| Аффилиация | Heilweil, Edwin J; Physics Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA |
| Аффилиация | Maslar, James E; Chemicals Science and Technology Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA |
| Аффилиация | Bendersky, Leonid A; Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA |
| Выпуск | 5 |
