Автор |
Abd-Alla, Mohamed, A. |
Автор |
Aly, Kamal, I. |
Дата выпуска |
1990 |
dc.description |
A novel method for the synthesis of copoly(ester-thioester)s of high molecular weight has been developed. These polymers were prepared readily by direct polycondensation of 4,4′-(terephthaloyldithio) diacetic acid I, 3,3′(isophthaloyldithio) diacetic acid II, or 1,8 (sebacoyldithio) diacetic acid III, with 2,6-bis(p-hydroxybenzylidene) cyclohexanone IV, and 2,6-divanillylidenecyclohexanone V, using a condensing agent consisting of a pyridine-thionyl chloride complex. The resulting polymers were characterized by elemental and spectral analyses, solubility, viscometry, differential scanning calorimetry and thermogravimetric analyses. The crystallinities of all the polymers were examined by X-ray diffraction. Several physical and thermal characteristics were correlated with their chemical structures. |
Издатель |
SAGE Publications |
Название |
Arylidene Polymers XIV—a New Synthetic Route to Copoly(ester-thioester)s by Direct Polycondensation of Thio-acids with Diarylidenecyclohexanone |
Тип |
Journal Article |
DOI |
10.1177/095400839000200403 |
Electronic ISSN |
1361-6412 |
Print ISSN |
0954-0083 |
Журнал |
High Performance Polymers |
Том |
2 |
Первая страница |
235 |
Последняя страница |
243 |
Аффилиация |
Abd-Alla, Mohamed, A., Polymer Laboratory 507, Department of Chemistry, Faculty of Science, Assiut University, Assiut, Egypt. |
Аффилиация |
Aly, Kamal, I., Polymer Laboratory 507, Department of Chemistry, Faculty of Science, Assiut University, Assiut, Egypt. |
Выпуск |
4 |
Библиографическая ссылка |
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Библиографическая ссылка |
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