| Автор | Creely, Joseph, J. |
| Автор | Conrad, Carl, M. |
| Дата выпуска | 1962 |
| dc.description | Previous x-ray diffraction studies of cellulose derivatives and other organic com pounds have shown that heat often has important effects, facilitating crystallization, transitions, and polymorphic transformations. However, the application of heat treat ments in conjunction with x-ray diffraction studies has usually been laborious, inexact, and at times ambiguous because of limitations of the technique. The present paper describes the adaptation of an x-ray furnace in conjunction with a two-pen potentiometer recorder and temperature-program controller to overcome some of the previous limita tions. A specially designed specimen holder is described. Thermal diffractograms of cellulose acetate and of benzyl and cyanoethyl cellulose are reproduced to demonstrate some of the advantages and possibilities of this technique. |
| Издатель | Sage Publications |
| Название | X-Ray Diffractometer Thermal Technique for Study of Structural Changes in Cellulosic Compounds1 |
| Тип | Other |
| DOI | 10.1177/004051756203200303 |
| Print ISSN | 0040-5175 |
| Журнал | Textile Research Journal |
| Том | 32 |
| Первая страница | 184 |
| Последняя страница | 189 |
| Аффилиация | Creely, Joseph, J., Southern Regional Research Laboratory,2 New Orleans 19, Louisiana |
| Аффилиация | Conrad, Carl, M., Southern Regional Research Laboratory,2 New Orleans 19, Louisiana |
| Выпуск | 3 |
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| Библиографическая ссылка | Conrad, C. M. and Creely, J. J., to be published. |
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