| Автор | Foreman, D.W. |
| Автор | Jakes, K.A. |
| Дата выпуска | 1993 |
| dc.description | Procedures were developed to enable standard x-ray diffractometric equipment to be used to study and compare textile fiber crystallographic characteristics. The approach was based on fitting diffractometric data to the Gaussian distribution by weighted regression analysis, which also supported an assessment of error propagation. Crystallite dimensions were obtained through the Scherrer method using analytically derived spectral line breadths. Percent crystalline component was determined by summing background-corrected amorphous and crystalline components of the spectra. A dif fractometric analysis was made of samples of rare textiles recovered from a 133-year old shipwreck, as well as modem fabrics submerged for three months at the same deep ocean site. The microcrystallite size of the historic textile materials increased, while the percent crystalline component decreased and unit cell dimensions remained con stant. The crystallite sizes of modern linen immersed for three months with iron, copper, or alone did not increase, while the percent crystalline component decreased and the unit cell dimensions remained constant. |
| Издатель | Sage Publications |
| Название | X-Ray Diffractometric Measurement of Microcrystallite Size, Unit Cell Dimensions, and Crystallinity: Application to Cellulosic Marine Textiles |
| Тип | Journal Article |
| DOI | 10.1177/004051759306300805 |
| Print ISSN | 0040-5175 |
| Журнал | Textile Research Journal |
| Том | 63 |
| Первая страница | 455 |
| Последняя страница | 464 |
| Аффилиация | Foreman, D.W., The Ohio State University, Columbus, Ohio 43110, U.S.A. |
| Аффилиация | Jakes, K.A., The Ohio State University, Columbus, Ohio 43110, U.S.A. |
| Выпуск | 8 |
| Библиографическая ссылка | Atalla, R.H. , The Crystallinity of Cellulosic Fibers, in "Preservation of Paper and Textiles of Historic and Artistic Value II," Advances in Chemistry Series, no. 193, J. C. Williams, Ed., American Chemical Society, Washington, D.C., 1981, pp. 69-176. |
| Библиографическая ссылка | Beers, Y., "Introduction to the Theory of Error," Addison-Wesley , New York, 1958. |
| Библиографическая ссылка | Berry, G.M., Hersh, S.P., Tucker, P.A., and Walsh, W.K., Reinforcing Degraded Textiles, Part I: Properties of Naturally and Artificially Aged Cotton Textiles, in "Preservation of Paper and Textiles of Historic and Artistic Value," Advances in Chemistry Series, no. 164, J. C. Williams, Ed., American Chemical Society, Washington, D.C., 1977 , pp. 228-248. |
| Библиографическая ссылка | Caulfield, D.F. , and Steffes, R.A., Water Induced Recrystallization of Cellulose , Tappi 52 (7), 1361-1366 (1969). |
| Библиографическая ссылка | Chidambareswaran, P.K., Sreenivasan,, S., and Patil, N.B., Quantitative Analysis of Crystalline Phases in Chemically Treated Cotton Fibers, Textile Res. J.57, 219-222 (1987). |
| Библиографическая ссылка | Conrad, J., Final Voyage, Am. Hist. Illustrated72 (3/4), 58-65 (1991). |
| Библиографическая ссылка | Foreman, D.W. , and Jakes, K.A., X-ray Diffractometric Measurement of Cellulose Microcrystallite Size, in "Cellulose '91 Proceedings ," Ellis Horwood, West Sussex, England (in press). |
| Библиографическая ссылка | Gröbe, A., Properties of Cellulose Materials, in "Polymer Handbook ," 3rd ed., J. Brandrup and E. H. Immergut, Eds., John Wiley & Sons, New York, 1989 , p. 117. |
| Библиографическая ссылка | Herdendorf, C.E., Discovery in an Alien EnvironmentAm. Hist. Illustrated72 (3/4), 66-71 (1991). |
| Библиографическая ссылка | Hermans, P.H. , and Weidinger, A., Quantitative X-ray Investigations on the Crystallinity of Cellulose Fibers, A Background Analysis , J. Appl. Phy. 19, 491 ( 1948). |
| Библиографическая ссылка | Hindeleh, A.M. , Crystallinity, Crystallite Size, and Physical Properties of Native Egyptian Cotton , Textile Res. J. 20, 667-674 (1980). |
| Библиографическая ссылка | Hindeleh, A.M. , and Johnson, D.J., The Resolution of Multipeak Data in Fiber Science, J. Phys. D. Appl. Phys. 4, 259-263 (1974). |
| Библиографическая ссылка | Hindeleh, A.M. , and Johnson, D.J., An Empirical Estimation of Scherrer Parameters for the Evaluation of True Crystallite Size in Fibrous Polymers , Polymer 21, 929-935 (1980). |
| Библиографическая ссылка | Jakes, K.A. , and Mitchell, J.C., On the Recovery and Drying of Textiles from a Deep Ocean Historic Shipwreck, J. Am. Ins. Cons. 31, 343-353 (1992). |
| Библиографическая ссылка | Jakes, K.A. , and Wang, W. The Characteristics of Textile Fibers and Fabrics Recovered from a Historic Deep Ocean Site, Ars Textrina ( in press). |
| Библиографическая ссылка | Jones, D.W., X-ray and Electron Diffraction, Cellulose I Structure Studies, in "Cellulose and Cellulose Derivatives," vol. V, N. Bikales, N. and L. Segal, Eds, Wiley-Interscience, New York, 1954, pp. 117-180. |
| Библиографическая ссылка | Kasper, J. S., and Lonsdale, K., Eds. "International Tables for Crystallography ," vol. II, Kynoch Press, Birmingham, England, 1967, p. 51. |
| Библиографическая ссылка | Khalifa, B.A. , Abdel-Zaher, N., Shoukr , F.S., Crystalline Character of Native Chemically Treated Saudi Arabian Cotton Fibers, Textile Res. J. 61, 602-608 (1991). |
| Библиографическая ссылка | Mann, J., Roldan-Gonzales, L., and Wellard, H.J., Crystalline Modifications of Cellulose, Part IV: Determination of X-ray Intensity Data, J. Polym. Sci.42, 165-171 (1960). |
| Библиографическая ссылка | Perel, J., AnX-ray Study of Regain-dependent Deformations in Cotton Crystallites, J. Textile Inst.81, 241-244 (1990). |
| Библиографическая ссылка | Pugh, E.M., and Winslow, G.H., "The Analysis of Physical Measurements," Addison-Wesley , Reading, MA, 1966. |
| Библиографическая ссылка | Rau, R.C., "Advances in X-ray Analysis," vol. V, Plenum Press, University of Denver, 1962, pp. 104-116. |
| Библиографическая ссылка | Ruland, W., X-ray Determination of Crystallinity and Diffuse Disorder Scattering , Acta Cryst. 14, 1180-1185 (1961 ). |
| Библиографическая ссылка | Scallan, A.M. , A Quantitative Picture of the Fringed Micellar Model of Cellulose, Textile Res. J. 41, 47-653 (1971). |
| Библиографическая ссылка | Scherrer, P. , Bestimmung der Grosse und inneren Struktur von Kolloidteilchen mittels Rontgenstrahlen, Nach. Ges. Wiss. Göttingen 2, 8-100 (1918). |
| Библиографическая ссылка | Segal, L., Creely, J.J., Martin, A.E., and Conrad, C.M., An Empirical Method for Estimating the Degree of Crystallinity of Native Cellulose Using the X-ray Diffractometer, Textile Res. J.29, 786-794 (1959). |
| Библиографическая ссылка | Shenouda, S.G., The Structure of Cotton Cellulose, in "Applied Fibre Science ," vol. 3, F. Happey , Ed., Academic Press Inc., NY, 1979, pp. 275-309. |
| Библиографическая ссылка | Tripp, V.W., and Conrad, C.M., X-ray Diffraction, in "Instrumental Analysis of Cotton Cellulose and Modified Cotton Cellulose," R. T. O'Connor , Ed., Marcel Dekker, Inc, NY , 1972, pp. 339-379. |
| Библиографическая ссылка | Varma, I.K. , Anantha Krishnan , S.R., and Krishnamoorthy, S., Effect of Chemical Treatment on Density and Crystallinity of Jute Fibers, Textile Res. J. 59, 368-370(1989). |
| Библиографическая ссылка | Wakelin, J.H. , Virgin, H.S., and Crystal, E., Development and Comparison of Two X-ray Methods for Determining the Crystallinity of Cotton Cellulose , J. Appl. Phys. 30, 1654-1662 (1959 ). |
| Библиографическая ссылка | Ward, K., Crystallinity of Cellulose and Its Significance for the Fiber Properties , Textile Res. J. 20, 363-372 (1950). |
| Библиографическая ссылка | Warren, B.E. , and Briscoe, J., The Structure of Silica Glass by X-ray Diffraction Studies, J. Am. Ceram. Soc. 21, 49-54 (1938). |
| Библиографическая ссылка | Young, H.D., "Statistical Treatment of Experimental Data," McGraw-Hill , New York, 1962. |
