Автор |
F N H Robinson |
Дата выпуска |
1982-08-01 |
dc.description |
The paper describes the design, construction and performance of a continuous-wave spectrometer for use at temperatures between 77K and 80 degrees C. The limiting sensitivity for chlorine resonances with narrow lines is 1 mu mol and compounds of molar volume up to 10<sup>4</sup> cm<sup>3</sup> can be studied. The corresponding figures for nitrogen resonances are 300 mu mol and 10<sup>3</sup> cm<sup>3</sup>. The continuous tuning range with a single coil is 2.5:1 and the resolution is a few PPM. It uses bisymmetric Zeeman modulation, there are no critical adjustments and no elaborate extra equipment is required. |
Формат |
application.pdf |
Издатель |
Institute of Physics Publishing |
Название |
A sensitive nuclear quadrupole resonance spectrometer for 2-60 MHz |
Тип |
paper |
DOI |
10.1088/0022-3735/15/8/005 |
Print ISSN |
0022-3735 |
Журнал |
Journal of Physics E: Scientific Instruments |
Том |
15 |
Первая страница |
814 |
Последняя страница |
823 |
Аффилиация |
F N H Robinson; Clarendon Lab., Univ. of Oxford, Oxford, UK |
Выпуск |
8 |