A high vacuum large volume specimen chamber for an electron microscope
R B Marcus; T T Sheng; C J Calbick; R B Marcus; Bell Telephone Labs. Inc., Murray Hill, NJ, USA; T T Sheng; Bell Telephone Labs. Inc., Murray Hill, NJ, USA; C J Calbick; Bell Telephone Labs. Inc., Murray Hill, NJ, USA
Журнал:
Journal of Physics E: Scientific Instruments
Дата:
1972-03-01
Аннотация:
A high-vacuum specimen chamber was constructed for a Siemens electron microscope in order that in situ studies of the growth of refractory metal films may be performed under clean well-defined conditions. The chamber is differentially pumped and reaches a vacuum of 0.1 mu Torr with the rest of the column at about 20 mu Torr. The hydrocarbon contamination rate at the specimen is approximately 2.5 AA min<sup>-1</sup> compared with about 500 AA min<sup>-1</sup> for the unmodified instrument. The stage operates smoothly, and images at 80000* are steady and free from vibration.
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