Автор |
Basak, Soubir |
Автор |
Tiwari, Vinay |
Автор |
Fan, Jinda |
Автор |
Achilefu, Samuel |
Автор |
Sethi, Virendra |
Автор |
Biswas, Pratim |
Дата выпуска |
2011 |
dc.description |
Abstract |
dc.description |
A single step gas phase method was developed to synthesize silica-coated iron oxide nanocomposite materials in a furnace aerosol reactor (FuAR) using premixed precursors. Synthesis of single component silica and magnetic iron oxide was studied to understand the decomposition mechanism of the precursors, identify the product crystal phase, and optimize the viable operating conditions for the controlled synthesis of nanocomposite material with desirable crystal phase, size, and morphology. The single component decomposition results are further extended to synthesize silica-coated magnetic iron oxide nanocomposite material using premixed precursor. A mechanism was proposed to explain the formation of SiO<sub>2</sub>-coated γ-Fe<sub>2</sub>O<sub>3</sub> nanocomposite in a single step in a FuAR based on chemical kinetics and was verified by supporting characterization results. The synthesized magnetic γ-Fe<sub>2</sub>O<sub>3</sub>/SiO<sub>2</sub> nanocomposite material was further tested for suspension stability, magnetic properties, and surface reactivity and was compared with uncoated γ-Fe<sub>2</sub>O<sub>3</sub> nanoparticles to demonstrate improved surface properties. |
Формат |
application.pdf |
Издатель |
Cambridge University Press |
Копирайт |
Copyright © Materials Research Society 2011 |
Тема |
Biomaterial |
Тема |
Core/shell |
Тема |
Nanostructure |
Название |
Single step aerosol synthesis of nanocomposites by aerosol routes: γ-Fe<sub>2</sub>O<sub>3</sub>/SiO<sub>2</sub> and their functionalization |
Тип |
research-article |
DOI |
10.1557/jmr.2011.97 |
Electronic ISSN |
2044-5326 |
Print ISSN |
0884-2914 |
Журнал |
Journal of Materials Research |
Том |
26 |
Первая страница |
1225 |
Последняя страница |
1233 |
Аффилиация |
Basak Soubir; Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, St. Louis,Missouri 63130 |
Аффилиация |
Tiwari Vinay; Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, St. Louis, Missouri 63130; and Center for Environmental Science and Engineering, Indian Institute of Technology, Mumbai 400076, India |
Аффилиация |
Fan Jinda; Department of Radiology, Mallinckrodt Institute of Radiology, Washington University School of Medicine, St. Louis, Missouri 63110 |
Аффилиация |
Achilefu Samuel; Department of Radiology, Mallinckrodt Institute of Radiology, Washington University School of Medicine, St. Louis, Missouri 63110 |
Аффилиация |
Sethi Virendra; Center for Environmental Science and Engineering, Indian Institute of Technology, Mumbai 400076, India |
Аффилиация |
Biswas Pratim; Department of Energy, Environmental and Chemical Engineering, Washington University in St. Louis, St. Louis, Missouri 63130 |
Выпуск |
10 |