| Автор | Yu, Tao |
| Автор | Li, Jin-Chai |
| Автор | Cai, Feng-Xin |
| Автор | Fan, Xiang-Jun |
| Автор | Chen, Ming-Sheng Ye Rong |
| Автор | Wu, Wan |
| Автор | Xiao, Nian |
| Автор | Tian, De-Cheng |
| Автор | Zhao, Wen-Kuan |
| Автор | Fang, You-Ling |
| Автор | Kuang, Ai-Yan |
| Дата выпуска | 1994 |
| dc.description | AbstractA new homemade are fullerene generator used in this experiment is reported. The comparation of yields of fullerenes (C<sub>60</sub>/C<sub>70</sub> mixture) was studied by different power supplies (AC and DC), different gaps of two graphite rods and different He pressure between 0.4×10<sup>4</sup>- 2.8×10<sup>4</sup> Pa. In our experiment, the highest yield up to 13% was achieved, when DC discharge was used and the optimum He pressure was near 0.8×10<sup>4</sup> - 1.6×10<sup>4</sup> Pa.The mixed fullerene was analyzed by electron impact masa spectnun (EIMS). The relative amount af C<sub>60</sub> to C<sub>70</sub> was 4.2 to 1. After column chromatography aeperation with hexane on alumina, 99.9% Cso was obtained. FTIR and <sup>1a</sup>C-NMR epectrum were ueed to characterize the pure C<sub>60</sub> samples. |
| Формат | application.pdf |
| Издатель | Taylor & Francis Group |
| Копирайт | Copyright Taylor and Francis Group, LLC |
| Тема | fullerene |
| Тема | yield |
| Тема | helium pressure |
| Название | A Study of Fullerene Preparation Technique |
| Тип | research-article |
| DOI | 10.1080/15363839408009548 |
| Print ISSN | 1064-122X |
| Журнал | Fullerene Science and Technology |
| Том | 2 |
| Первая страница | 223 |
| Последняя страница | 231 |
| Аффилиация | Yu, Tao; Department of Physics, Wuhan University |
| Аффилиация | Li, Jin-Chai; Department of Physics, Wuhan University |
| Аффилиация | Cai, Feng-Xin; Department of Physics, Wuhan University; Department of Physics, Henan University |
| Аффилиация | Fan, Xiang-Jun; Department of Physics, Wuhan University |
| Аффилиация | Chen, Ming-Sheng Ye Rong; Department of Physics, Wuhan University |
| Аффилиация | Wu, Wan; Department of Physics, Wuhan University |
| Аффилиация | Xiao, Nian; Department of Physics, Wuhan University |
| Аффилиация | Tian, De-Cheng; Department of Physics, Wuhan University |
| Аффилиация | Zhao, Wen-Kuan; Department of Chemistry, Wuhan University |
| Аффилиация | Fang, You-Ling; Department of Chemistry, Wuhan University |
| Аффилиация | Kuang, Ai-Yan; Department of Chemistry, Wuhan University |
| Выпуск | 3 |
| Библиографическая ссылка | Kroto, H. W. 1985. Nature, 318: 162 |
| Библиографическая ссылка | Kraschmer, W. 1990. Chem. Phys. Lett., 170: 167 |
| Библиографическая ссылка | Kraschmer, W. 1990. Nature, 347: 354 |
| Библиографическая ссылка | Parker, D. H. 1991. J. Am. Chem. Soc., 113: 7499 |
| Библиографическая ссылка | Taylor, R. 1990. J. Chem. Soc. Chem. Commum., : 1423 |
| Библиографическая ссылка | Aije, H. 1990. J. Phys. Chem., 94: 8630 |
| Библиографическая ссылка | Haufler, R. E. 1990. J. Phys. Chem., 94: 8634 |
| Библиографическая ссылка | Hare, J. P. 1991. Chem. Phys. Lett., 177: 394 |
