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Автор Pietrzyk, Donald J.
Автор Cahill, William J.
Дата выпуска 1982
dc.description AbstractAmberlite XAD-4, a nonpolar adsorbent with a particle size of 62 to 177 μm, was packed into 58 mm i.d. x 294 mm columns and radially compressed in the Waters Prep 500 preparative liquid chromatograph. Efficiency, loading capacity (multigram samples), resolution, recovery, and types of mobile phases were major parameters studied. Since XAD-4 is chemically inert mixed solvent and pH control from 1 to 13 can be successfully used in the mobile phase. Separations illustrating these advantages and the scope of the 58 mm i.d. column are described.
Формат application.pdf
Издатель Taylor & Francis Group
Копирайт Copyright Taylor and Francis Group, LLC
Название Amberlite XAD-4 as a Stationary Phase for Preparative Liquid Chromatography in a Radially Compressed Column
Тип research-article
DOI 10.1080/01483918208060586
Print ISSN 0148-3919
Журнал Journal of Liquid Chromatography
Том 5
Первая страница 781
Последняя страница 795
Аффилиация Pietrzyk, Donald J.; The University of Iowa, Chemistry Department
Аффилиация Cahill, William J.; The University of Iowa, Chemistry Department
Выпуск 4
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Библиографическая ссылка Pietrzyk, D. J. and Stodola, J. D. 1981. Preparative Liquid Chromatography of 1:1 Adducts Derived from the Reaction of Malondialdehyde with Amino Acids. Anal. Biochem., 117: 245–249.
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