| Автор | McManus, S. P. |
| Автор | Carroll, J. T. |
| Автор | Grohse, P. M. |
| Автор | Pittman, C. U. |
| Дата выпуска | 1969 |
| Формат | application.pdf |
| Издатель | Taylor & Francis Group |
| Копирайт | Copyright Taylor and Francis Group, LLC |
| Название | 2-SUBSTITUTED-5-METHYL-2-OXAZOLINES |
| Тип | research-article |
| DOI | 10.1080/00304946909458377 |
| Print ISSN | 0885-6672 |
| Журнал | Organic Preparations and Procedures |
| Том | 1 |
| Первая страница | 183 |
| Последняя страница | 186 |
| Аффилиация | McManus, S. P.; Department of Chemistry, University of Alabama in Huntsville |
| Аффилиация | Carroll, J. T.; Department of Chemistry, University of Alabama in Huntsville |
| Аффилиация | Grohse, P. M.; Department of Chemistry, University of Alabama in Huntsville |
| Аффилиация | Pittman, C. U.; Department of Chemistry, University of Alabama |
| Выпуск | 3 |
| Библиографическая ссылка | Acid-catalyzed Cyclization Reactions. V. For paper IV, see preceding paper (ref. 4) |
| Библиографическая ссылка | (a) Authors to whom inquiries should be addressed; (b) Acknowledgement is made for partial financial support from the Petroleum Research Fund, administered by the American Chemical Society, and from the National Aeronautics and Space Administration |
| Библиографическая ссылка | Petroleum Research Fund Undergraduate Scholar |
| Библиографическая ссылка | McManus, S. P., Carroll, J. T., Grohse, P. M. and Pittman, C. U. Jr. Org. Preps. and Proc., to be published |
| Библиографическая ссылка | Kay, P. 1893. Ber., 26: 2848 |
| Библиографическая ссылка | McManus, S. P., Carroll, J. T., Grohse, P. M., Taddei, C. R. and Pittman, C. U. Jr. 1968. 20th Annual Southeastern Regional Meeting, American Chemical Society. Dec.4–71968, Tallahassee, Florida. Abstracts p. 69; paper in preparation for publication |
| Библиографическая ссылка | Other acids have been successfully used and no attempt here is made to show the particular acid media where the yield is maximized for each amide |
| Библиографическая ссылка | Wenker, H. 1935. J. Am. Chem. Soc., 57: 1079 |
| Библиографическая ссылка | Seeliger, W., Aufderhaar, E., Diepers, W., Feinauer, R., Nehring, R., Thier, W. and Hellman, H. 1966. Angew Chem. Internat. Edit., 5: 875 |
| Библиографическая ссылка | All of the benzamides were prepared by the Schotten-Baumann procedure.<sup>10</sup> N-allylacetamide was prepared using ketene.<sup>4</sup> The allylamine used was Eastman “white label”. The following derivatives of N-allylbenzamide have not previously been reported: p-CH<sub>3</sub>, m.p. 75.5–76.5°, Anal. Calc.: N, 7.99, Found: 7.72; p-F, m.p. 67–68°, Anal. Calc.: N, 7.90, Found: 7.68; p-NO<sub>2</sub>, m.p. 118–118.5°, Anal. Calc.: N, 13.59, Found: 13.37; p-(CH<sub>3</sub>)<sub>2</sub>N, m.p. 131–132°, Anal. Calc.: N, 13.71, Found: 13.98; p-CH<sub>3</sub>O, m.p. 42.5–43.5°, Anal. Calc.: N, 7.32, Found: 7.40. The i.r. and n.m.r. spectra of all new compounds were consistant with the assigned structures |
| Библиографическая ссылка | Vogel, A. I. 1956. “Textbook of Practical Organic Chemistry”, , 3rd Edition, 582London: Longmans. |
| Библиографическая ссылка | If conversion is complete, it is unnecessary to extract the solution while it is slightly acidic. Since hydrolysis of the 2-oxazolines is fairly rapid in some acidic media, exposure to dilute solutions is avoided where possible. See footnote a in the Table |
| Библиографическая ссылка | Bassiri, T. G., Levy, A. and Litt, M. 1967. Polymer Letters, 5: 871 |
| Библиографическая ссылка | Olah, G. A. and Pittman, C. U. Jr. 1966. “Advances in Physical Organic Chemistry”, Edited by: Gold, V. Vol. 4, 305New York: Academic Press. |
